{"id":2815,"date":"2016-12-15T07:48:48","date_gmt":"2016-12-15T04:48:48","guid":{"rendered":"http:\/\/pharmacy.uokerbala.edu.iq\/wp\/test\/2016\/12\/15\/determination-asprien-by-high-performance-liquid-chromatography-hplc\/"},"modified":"2016-12-15T07:48:48","modified_gmt":"2016-12-15T04:48:48","slug":"determination-asprien-by-high-performance-liquid-chromatography-hplc","status":"publish","type":"post","link":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/blog\/2016\/12\/15\/determination-asprien-by-high-performance-liquid-chromatography-hplc\/","title":{"rendered":"Determination Asprien by High Performance Liquid chromatography (HPLC)"},"content":{"rendered":"<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\">Determination Asprien by High Performance Liquid chromatography (HPLC)<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\">Semaa\u00a0 Hamed\u00a0 Ahmad<sup>(1)<\/sup> .<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\">Department of Maintenance and Restoration \u2013 College of Archaeology \u2013 University of Samarra \u2013 Samarra \u2013 Iraq<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\"><strong>Received\u00a0 <\/strong>(January)<strong> , Accepted <\/strong>(June).<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\"><strong>\u00a0<\/strong><\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\"><strong>Abstract :<\/strong><\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\">This research in includes determination Asprien by using high Liquid\u00a0 chromategraphitic\u00a0 technique by using Licrosorb C-<sub>18<\/sub> column, That studies to quantitative estimate The study is organic rate in dynamic and component from regular solution (0.02 sodium acetate) at pH=7\u00a0 The study rate is dynamic flow (1 ML\/Min) .<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\">The linearity of concentration (0.1-0.001)M and correlation coefficient ( 0.9926) The relative standard deviation RSD % (0.49-0.72) and detection Limits were (0.1) M and percent relative errors were (1.20-1-0.60) respectively with percent recovery ranged (93-96)%\u00a0 .<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\"><strong>\u062a\u0642\u062f\u064a\u0631 \u0627\u0644\u0627\u0633\u0628\u0631\u064a\u0646 \u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0643\u0631\u0648\u0645\u0627\u062a\u063a\u0631\u0627\u0641\u064a\u0627 \u0627\u0644\u0633\u0627\u0626\u0644 \u0630\u0627\u062a \u0627\u0644\u0627\u062f\u0627\u0621 \u0627\u0644\u0639\u0627\u0644\u064a<\/strong><\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\"><strong>\u0633\u064a\u0645\u0627\u0621 \u062d\u0645\u064a\u062f \u0623\u062d\u0645\u062f<\/strong><\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\">\u00a0<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\"><strong>\u0627\u0644\u062e\u0644\u0627\u0635\u0629\u00a0 \u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 <\/strong><\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\">\u00a0\u00a0\u00a0\u00a0 \u064a\u062a\u0636\u0645\u0646 \u0627\u0644\u0628\u062d\u062b \u062a\u0642\u062f\u064a\u0631 \u0627\u0644\u0623\u0633\u0628\u0631\u064a\u0646 \u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u062a\u0642\u0646\u064a\u0629 \u0643\u0631\u0648\u0645\u0627\u062a\u063a\u0631\u0627\u0641\u064a\u0627 \u0627\u0644\u0633\u0627\u0626\u0644 \u0630\u0627\u062a \u0627\u0644\u0627\u062f\u0627\u0621 \u0627\u0644\u0639\u0627\u0644\u064a \u0648\u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u0627\u0644\u0639\u0645\u0648\u062fC-<sub>18<\/sub> \u00a0\u062f\u0631\u0627\u0633\u0629 \u0627\u0644\u0638\u0631\u0648\u0641 \u0627\u0644\u0645\u062b\u0644\u0649 \u0644\u0644\u062a\u0642\u062f\u064a\u0631 \u0627\u0644\u0643\u0645\u064a \u0645\u0646 \u062d\u064a\u062b \u062f\u0631\u0627\u0633\u0629 \u0646\u0633\u0628\u0629 \u0627\u0644\u0645\u062d\u0648\u0631 \u0627\u0644\u0639\u0636\u0648\u064a \u0641\u064a \u0627\u0644\u0637\u0648\u0631 \u0627\u0644\u0645\u062a\u062d\u0631\u0643 \u0648\u0627\u0644\u0645\u0643\u0648\u0646 \u0645\u0646 \u0645\u062d\u0644\u0648\u0644 \u0645\u0646\u062a\u0638\u0645 (0.02 \u0645\u0648\u0644\u0627\u0631\u064a \u0645\u0646 \u062e\u0644\u0627\u062a \u0627\u0644\u0635\u0648\u062f\u064a\u0648\u0645) \u0639\u0646\u062f \u00a0PH= 7\u060c \u0648\u062f\u0631\u0627\u0633\u0629 \u0645\u0639\u062f\u0644 \u0633\u0631\u0639\u0629 \u062c\u0631\u064a\u0627\u0646 \u0627\u0644\u0637\u0648\u0631 \u0627\u0644\u0645\u062a\u062d\u0631\u0643 (1 \u0645\u0644 \/ \u062f\u0642\u064a\u0642\u0629)\u00a0 \u0648\u0643\u0627\u0646\u062a \u062e\u0637\u064a\u0629 \u0627\u0644\u062a\u0631\u0627\u0643\u064a\u0632 (0.001-0.1) \u0645\u0648\u0644\u0627\u0631\u064a \u060c \u0648\u0628\u0645\u0639\u0627\u0645\u0644 \u0627\u0631\u062a\u0628\u0627\u0637 0.9926 \u060c \u0648\u0627\u0644\u0646\u062a\u0627\u0626\u062c \u0627\u0644\u0627\u062d\u0635\u0627\u0626\u064a\u0629 \u0627\u0644\u062a\u062d\u0644\u064a\u0644\u064a\u0629 \u0628\u064a\u0646\u062a \u0627\u0646 \u0645\u0639\u062f\u0644 \u0627\u0644\u0627\u0646\u062d\u0631\u0627\u0641 \u0627\u0644\u0642\u064a\u0627\u0633\u064a \u0627\u0644\u0646\u0633\u0628\u064a RSD % (0.49-0.72) \u060c \u0648\u0627\u0644\u062e\u0637\u0623 \u0627\u0644\u0646\u0633\u0628\u064a (1.20-1-0.60) \u0648\u062d\u062f \u0643\u0634\u0641 (0.1) \u0645\u0648\u0644\u0627\u0631\u064a \u060c \u0648\u0628\u0645\u0639\u062f\u0644 \u0627\u0633\u062a\u0631\u062c\u0627\u0639 (93-96)% .<\/span><\/p>\n<p dir=\"rtl\" style=\"text-align: center;\">\u00a0<\/p>\n<p dir=\"rtl\" style=\"text-align: center;\"><span style=\"font-size: 12pt;\"><strong>\u062a\u062d\u0645\u064a\u0644 \u0627\u0644\u0628\u062d\u062b \u00a0<a href=\"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/wp-content\/uploads\/sites\/6\/2016\/12\/images_journal_no.11_11%2833%29.pdf\" target=\"_blank\" rel=\"alternate\"><img data-recalc-dims=\"1\" loading=\"lazy\" decoding=\"async\" class=\" size-full wp-image-2408\" src=\"https:\/\/i0.wp.com\/pharmacy.uokerbala.edu.iq\/wp\/wp-content\/uploads\/sites\/6\/2015\/01\/images_adobe-pdf-logo.png?resize=35%2C35&#038;ssl=1\" alt=\"\" width=\"35\" height=\"35\" \/><\/a><\/strong><\/span><\/p>\n","protected":false},"excerpt":{"rendered":"<p>Determination Asprien by High Performance Liquid chromatography (HPLC) Semaa\u00a0 Hamed\u00a0 Ahmad(1) . Department of Maintenance and Restoration \u2013 College of<\/p>\n","protected":false},"author":7,"featured_media":2408,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_monsterinsights_skip_tracking":false,"_monsterinsights_sitenote_active":false,"_monsterinsights_sitenote_note":"","_monsterinsights_sitenote_category":0,"_jetpack_memberships_contains_paid_content":false,"footnotes":""},"categories":[1],"tags":[],"class_list":["post-2815","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-1"],"jetpack_featured_media_url":"https:\/\/i0.wp.com\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-content\/uploads\/sites\/6\/2015\/01\/images_adobe-pdf-logo.png?fit=35%2C35&ssl=1","jetpack_sharing_enabled":true,"_links":{"self":[{"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/posts\/2815","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/users\/7"}],"replies":[{"embeddable":true,"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/comments?post=2815"}],"version-history":[{"count":0,"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/posts\/2815\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/media\/2408"}],"wp:attachment":[{"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/media?parent=2815"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/categories?post=2815"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/pharmacy.uokerbala.edu.iq\/wp\/en\/wp-json\/wp\/v2\/tags?post=2815"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}